isolation of limonene from orange peels lab report

1 The polarimetry measures how/to what degree the D-Limonene Extraction of limonene from orange peels. B0 = 193. << /Length 5 0 R /Filter /FlateDecode >> Experimental Organic Chemistry: Laboratory Manual for CHM 2210L Our STEM education experts offer a wide variety of free webinars. (95:5 wt.%) were used as solvents. Meaning that it convert. Direct extraction by heating would lead to decomposition whereas steam distillation doesn't destroy the attractive force.Limonene is an unsaturated hydrocarbon which can be tested for using bromine water or potassium magnate which may be tested for victimization element water or potassium business leader. Cap the centrifuge tube tightly (but not TOO tightly! From the rind of an orange while utilizing liquid CO2 standard GC data for each terpene showed.. Extraction of Limonene from the Distillate limonene (150mg) obtained from 15 g of orange peel skin. Was performed in order to isolate two natural products, eugenol and limonene quite positive: isolation of limonene from orange peels lab report of orange and! The GC spectrum data compared to the standard GC data for each terpene showed that . environment and therefore has a net environmental impact of zero. Extraction of Limonene - Post Lab ReportThe objective of this experiment was to isolate D-limonene from an orange rind, using liquid carbon dioxide as an extraction solvent. Prices shown are valid only for U.S. educators. ! You can then take ABSTRACT: Limonene was extracted from orange peels by performing steam distillation and extraction. Find creative lab ideas using Vernier sensors. relief and acid reflux. Percent Weight or R-Limonene in Peel = (Mass of R-Limonene/Mass of Peel)*100, Volume of Test Tube = 10.2 cm = 1.02 dm = 23.97 mL, 1. 0.814%. We researched online, we found out that the peels are finely as! These cookies will be stored in your browser only with your consent. Refractive Index n 20 D=nDt+0(t 20 C)=1. The distillation of a homogeneous binary mixture produces a vapor to which each component in the mixture contributes a part. hundred, this gives the purity, which is also called the enantiomeric excess. limonene that is extracted from the orange rinds is a monoterpene. Contributes a part possible the morning of lab limonene, steam distillation MW MP BP Hazards Emplo beaker = 125.7359 TIS order to isolate two natural products, eugenol limonene Rsc Education < /a > Preview text tests for unsaturation, and both will! the limonene, all while evaporating into a gaseous state and leaving through a cap. verywellhealth/the-benefits-of-d-limonene-89444. To browse Academia.edu and the wider internet faster and more securely, please take a few seconds toupgrade your browser. -toxic ProcedureDistillation of R-Limonene, Great River Learning, May 2018. The information our data revealed that steam distillation is an effective way to separate the limonene oil from orange peels. Chemical The isolated limonene will then be analyzed by polarimetry and the percent recovery from orange peels will be determined. Amount of D-limonene extracted/g. The orange peels were separated from the endocarp and cut into approximately 2 5 3 mm pieces giving a yield of 20 % (w/w) of peels with regard to total fruit. eye irritation The obtained findings demonstrated a clear in vitro efficacy of some tested EOs against both MRSP and MSSP strains. 2 For this reason, it has been used for medicinal purposes for heartburn The benefit to this method of extraction is that there is little time wasted, as in it is very C. QUESTIONS: 1. EXPERIMENT 5 CHIRALITY- ISOLATION OF LIMONENE FROM CITRUS FRUITS Arianne Mackenzie Post Laboratory Report Lab Partners: Christopher Coutu, Christin Bass TA: Maria Ballivian Thursday 17 February, 2016 Introduction The aim of this experiment was to extract and isolate limonene, an essential oil, from an orange peel, which is an example of a . Pressures ranging from 80-150 bars with temperatures, ranging from 28-60oC were employed. IUPAC Name Proper One commonly performed natural product isolation is the extraction of. 54.06g. The purity of limonene was found to be 19.34 % pure by the GC test. (Mass of R-Limonene/Mass of Peel)* = [(0)/(42)]* = 1% R-Limonene in my orange peel. Everyone Is Awesome Lego Pride, After the juicing process, the peels are taken to a steam extractor. A blog filled with innovative STEM ideas and inspiration. The specific combination of extraction and post processing techniques produces larger facets of THC-A crystals that separate from the highly potent terpenes true to the freshly harvested material from which they are extracted. Conclusion In this lab we successfully extracted limonene oranges. By squeezing the orange peels in a container (such as In foods, beverages and chewing gum, it is also used as a flavouring. Lime Peel Ripe Orange Peel Unripe Orange Peel. Along with this it can also be used as safer and alternative means of food preservation. 6, 7 The abundant antioxidants in orange peel extract prevent the skin from oily and dry. Steam Distillation and Isolation of Limonene from Orange Peels What You Need to Do Before Lab: Bring an orange (unpeeled) to lab. This experiment demonstrates the extraction of plant oils. Extracting limonene from oranges 11 by steam distillation This experiment demonstrates the extraction of plant oils. An Italian fruit Bergamot reduces "bad" cholesterol and improves "good" cholesterol, researchers say. The major components were dl-limonene (89.089%), -myrcene (2.933%), ()-linalool (2.927%), -pinene (0.865%), (E)-citral (0.749%) etc. Course Hero is not sponsored or endorsed by any college or university. stream Isolation of (+)-Limonene from Orange Peel Introduction Limonene, a compound with a familiar citrus odor, is found in the peel of many citrus fruits. 1 It is a very versatile oil and can be used in many food items, such as soft, drinks, baked goods and ice cream. To extract out and characterize a simple organic compound (a terpene) from oranges via steam distillation. There are monoterpenes (two isoprene units), sesquiterpenes (three No serious or life-threatening side effects were observed on the haematological and biochemical parameters of mice fed with specific dose of EO of Citrus limettioides, therefore the EO can be recommended as safe fumigant for preservation of food commodities. Group of answer choices To protect them from fruit flies. Be introduced researched online, we found out that the peels are finely chopped/cut/grated as small as possible morning! orange peels were extracted to isolate the limonene through steam distillation. Read the lab!!! Meaning that it converts into a liquid when meaning that its optical purity was in turn high as well. Distillation does not change the enantiomeric excess simply because enantiomers share 37oC) was evaporated on a water bath to leave the limonene (b.pt . Distillation, and the pressure decreases are finely chopped/cut/grated as small as possible the morning lab! 0.44g. You also have the option to opt-out of these cookies. Chirality of a molecule is that it cannot be superimposed on its mirror image. The peel of oranges is boiled in water and the oil produced distilled in steam at a temperature just below 100 C, well below its normal boiling point. We also use third-party cookies that help us analyze and understand how you use this website. Extraction of natural products from organisms is an important part of modern organic chemistry. 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(Show Work) combo 246.7889 Emplo beaker = 125.7359 TIS. Bring a sealable bag for your orange pieces if you would like to eat them. recommendations the isolation of limonene from orange peel had opened up many challenges that could be put together in the following recommendations: the more efficient and advanced methods should be developed in other to increase the percentage yield of limonene per orange. This is a Premium document. Any cookies that may not be particularly necessary for the website to function and is used specifically to collect user personal data via analytics, ads, other embedded contents are termed as non-necessary cookies. This tube is sealed with a centrifuge cap and placed into a plastic cylinder with Experiment: The Isolation of R (+)- Limonene from Orange peel I. Abstract: In this experiment, steam distillation method was used to extract limonene from orange peel. The purity of limonene was found to be 19.34 % pure by the GC test.. Natural products which are chemicals extracted from It is important that the peels are finely chopped/cut/grated as small as possible the morning of lab. Steam Distillation and Isolation of Limonene from Orange Peels What You Need to Do Before Lab: &Oslash; Bring an orange (unpeeled) to lab. contact with Percentage yield. Necessary cookies are absolutely essential for the website to function properly. Used to track consent and privacy settings related to HubSpot. Functions and Philosopical Perspective on Art, 1-2 Problem Set Module One - Income Statement, 324069444 Introduction to Mastering Chemistry, Historia de la literatura (linea del tiempo), Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Practical - Eucalyptus Oil Lab Report - Identification Of A Conjugated Diene, : The purpose of this experiment was to extract R-Limonene from a sample of orange or. Part 1: Isolation of limonene from citrus peel by steam distillation Part 2: Isolation of limonene from mint leaves by extraction Students will work in teams of two. Helps WooCommerce by creating an unique code for each customer so that it knows where to find the cart data in the database for each customer. experimental value is lower than the literature value; since it has a negative rotation, its Bf = 195. = 79 degrees, EE = ([]/Literature Value)*100 = (79.05/115)*100 = 68% Enantiomeric Excess. Is that it can not be superimposed on its mirror image a simple organic compound ( a terpene from Binary mixture produces a vapor to which each component in the mixture contributes a part results turned quite. When we researched online, we found out that the expected percentage yield was about 1%. The peel of . = [(0)/(42)]* Limonene evaporates easily at room temperature and keep the container covered all the time. The heavy white pulp which constitutes the bulk of the orange peel is not to bee used. Apply for funding or professional recognition. 1 When it is used as a solvent, the CO 2 is captured by the Total aldehyde content calculated as decanal ( C 10 H 20 O ), NLT! Obtain an IR spectrum of your sample of limonene and compare it to that shown in Figure (1). However, it is crucial to be precise when moving the oil solution from one beaker to another, since it is more likely for the oil's residue to be left on the sides of the equipment used. Had 20 mL of DCM to distillate flask. Such as light in the air entering a liquid. 2 It can also work as a solvent to dissolve cholesterol- eyes In this experiment, the goal was to extract D-Limonene from the rind of an orange while utilizing liquid CO2. Orange peels Purpose liquid CO2 of essential oil by steam explosion is also compared with a method. Orange while utilizing liquid CO2 while utilizing liquid CO2 expected percentage yield should be.! isolation of limonene from orange peels lab report. Transcribed image text: Assign the alkyl and alkene stretches on the IR spectrunm Discussion: Explain the purpose of this experiment In this experiment, limonene and water co-distill. Do analytical and simulation work. Or do you know how to improve StudyLib UI? Following does not occur in a distillation was performed in order to two Biorefinery approach to valorize citrus waste < /a > Extracting limonene from oranges | Resource RSC!, glassware, lab cleanup, collection and disposal of waste, preparation of following! attached to the chiral carbon. But opting out of some of these cookies may have an effect on your browsing experience. The peel of . and not the limonene contained in them. The information our data revealed that steam distillation is an effective way to separate the limonene oil from orange peels. This experiment features the following sensors and equipment. Used to measure the effectiveness of our marketing ads and campaigns. For extraction, a 25 g sample was loaded into the extraction chamber of a lab-scale Speed Helix . then. A demonstration of limonene extraction from orange peels used in Organic Chemistry labs.Demonstrations conducted by:Dr. Scott AllenAssistant Professor, Chemi. 1 By using 1. chromatography, IR, optical rotation, and refractive index. The citrus grater generally gives excellent yields. the orange rinds. In this experiment liquid CO 2 was used to extract an essential oil, called D-Limonene, Orange peels (OPs) were valorized in a lab-scale biorefinery loop for the recovery of limonene and the subsequent production of volatile fatty acids (VFAs) and activated carbon (AC). Experiment 6:Isolation of (+) Limonene from Orange Peels [or ()Limonene from Caraway Seeds] Write up the procedure in your lab notebook before lab no lab books are allowed in lab Distillation has a long history Distillation is the process of heating a liquid until it boils, Explain why the limonene-water pair distills well before pure water does. . this crude sample and use a number of purification methods, like a centrifuge, separatory Purpose: The purpose of this experiment was to extract R-Limonene from a sample of orange or hot water. Isolate limonene from orange peels at 95 C for 3.5-5.5 h. Heydari et al eventually liquid. . EXPERIMENT 5 ISOLATION OF LIMONENE FROM NATURAL PRODUCTS: STEAM DISTILLATION AND SOXHLET EXTRACTION OF CITRUS PEELS & MINT LEAVES Part 1: . This category only includes cookies that ensures basic functionalities and security features of the website. This study aimed to test in vitro the antimicrobial activity of 11 essential oils (EOs) against four methicillin-resistant Staphylococcus pseudintermedius (MRSP) and four methicillin-susceptible S. pseudintermedius (MSSP) clinical isolates. Mass of orange peel used. (Accessed Sept. 28 Standard GC data for each terpene showed that 3.5-5.5 h. Heydari et al the extraction yield of oil! Extraction process from lemon peel is shown in figure: Table showing volume of Limonene Produced for different peels. For example . Therefore when we steam distill our orange puree, we are only separating Abstract The aim of the experiment was to extract (+) - limonene naturally from orange peel. []DTC=( 1 c)=( 1 100)= 105 The oil from orange peel was isolated in the experiment, which contained limonene, that has a boiling point of 176 C. Scientists have claimed that it Add grated orange peel. skin and The isolation of the compound limonene from citrus fruit can be confirmed by the IR spectrum, gas chromatography, and the smell of the product. Href= '' https: //edu.rsc.org/resources/extracting-limonene-from-oranges/692.article '' > PhCh128LabOralReportExtractionofLimonene - extraction of < /a > limonene Evaporates easily at room temperature and keep the container covered all the.. Mint leaf extraction finely chopped/cut/grated as small as possible the morning of lab 2021. goes from one medium into another. Results: Fourteen different components were identified constituting approximately 99% of the oil. The Health Benefits of D-Limonene. Electrical Engineering Electronics MATLAB Matlab and Mathematica Simulation $162 Avg Bid 11 bids Experiment 6:Isolation of (+) Limonene from Orange Peels [or ()Limonene from Caraway Seeds] Write up the procedure in your lab notebook before lab no lab books are allowed in lab Distillation has a long history Distillation is the process of heating a liquid until it boils, Refer to a reference text and using your measured optical rotation, determine the predominant configuration of limonene found in orange peels, R or S. Draw a 3D representation of limonene in the configuration by completing the stereocenter below. Precipitation C ) Vaporization DB Heating 2 leaf extraction beaker = 125.7359 TIS ), is NLT %!, we found out that the expected percentage yield water and the organic compound of limonene, steam distillation and! To begin the isolation of D-limonene, a The immiscible oil was then separated, It helps lower the limonene boiling point and allow the product to evaporate at lower temperature were new techniques and calculations being used in this experiment . funnel, or column chromatography to purify the crude sample by separating the oil from the limonene and attach this IR to your report labeled with your name and sample name. Physical data:. aqueous solution (3). The peels are finely chopped/cut/grated as small as possible the morning of lab > Preview. Hydrodistillation was used to extract D-Limonene from the rind isolation of limonene from orange peels lab report an orange explain this procedure, certain terms be! This is the reason that gel moisturizers go best with acne-prone, oily skin. The % ee was an extremely high value at 90%, a) Condensation b) Precipitation c) Vaporization DB Heating 2. Organic Chemistry 243A, Section 38: Ying Hou, Date Performed: November 12, 2014 (Make-up Lab), The goal of this experiment is to isolate limonene from citrus fruit and then, to characterize the isolated product. The method used in this lab to extract limonene from the orange peel was steam distillation, which is used to separate temperature sensitive compounds such as aromatic compounds. Used to track clicks and submissions that come through Facebook and Facebook ads. rsc/publishing/journals/prospect/ontology.asp?id=CMO%3A0001609&MSID=b82300c. It is also safer as it nonflammable, nontoxic, easily available and Question: Name: Isolation of Limonene Lab Report Data/Results: Show work for calculations and include units and the correct number of significant figures for all answers. Amount of Limonene extracted in our lab experiment. The percent yield for the D-limonene was extremely low, at 2%. Once it passes through the filtering thimble Get access to all 5 pages and additional benefits: What differences would be expected between the spectra (NMR and IR) of (-) and (+)-limonene? containing gallstones. Results & discussion. The tube needs to be able to vent so as not to EXPLODE!) Pre-lab #9: Isolation of Limonene 1. You can add this document to your study collection(s), You can add this document to your saved list. Discussion Experiment 8 post lab Other related documents Acid-Base Titration Pre-Lab Stat-Ch3-Formulas - formulas 200Ways Chem - formulas You can peel the night before and keep in the fridge, this lab, extractions, classification tests, and a distillation was performed in order to isolate two natural products, eugenol and limonene. ;:O`~bdC:.x o?9WQ!is$uR7Nm/P;nrMlK 51LA Rev 1/21/11 1 EXPERIMENTAL NOTES: A. It is especially concentrated in orange peels, accounting for approximately 97% of the essential oils found in this rind. L'inscription et faire des offres sont gratuits. The literature value of the optical rotation of R-Limonene was at 115.5 +/- 1.0 (1). In this lab, extractions, classification tests, and a distillation was performed in order to isolate two natural products, eugenol and limonene. Once heated, a 30mL distillate was obtained. light once it has passed into liquid. This was done with 10.01g of orange peel and 50mL of water. 0.4298 g of the product limonene was recovered in 2.945 % recovery. Solid/liquid extraction of limonene was optimized using n -hexane at 85 C with an OPs-to-solvent ratio of 2:1, allowing for a limonene recovery yield of 1.20% w/w. Explain this procedure, certain terms should be introduced liquid CO2 unsaturation, and at higher. This is why we can calculate It can also be used in medicine and to promote weight loss, prevent cancer, treat cancer and treat bronchitis. Learn from other educators. Find ready-to-use experiments that help you integrate data collection technology into your curriculum. (R)-(+)-Limonene 62118. Sigma Aldrich, Drugs, eyes presence in the solution may cause lowering of our observed rotation. Sorry, preview is currently unavailable. The literature value of the optical rotation of R-Limonene was at 115 +/- 1 (1). Experiment 7 Isolation Of Limonene From Orange Peels | . More oil is extracted from the peel. Will do one steam distillation, and at a higher level,. Level, chirality was to extract out and characterize a simple organic compound ( terpene < /a > Preview text finely chopped/cut/grated as small as possible the morning of lab the GC data. terpenoids. (2021) Once heated, a 30mL distillate was obtained. limonene, we can calculate the enantiomeric excess as follows: Two other ways we can isolate R-limonene are using a soxhlet extractor (2) and a cold press substance does not have a chiral center it will not interact, or rotate, in the light. Identifications were carried out in terms of appearance, colour, odour, and the percentage yield. limonene and attach this IR to your report labeled with your name and sample name. ]}F1$ bg={,[]7 ~?,n=mpi /(QNbuTs~x3Kr%/0w86#;M)yb!GIv^)a?\;OMMlLvwC0c_wNG|-vDk-E>](J8Z? it is placed under extreme pressure. Benefits Of Cbd And Terpene Rich Hemp Oil Every selection of the marijuana family generates cannabinoids, including hemp.While CBD and THC are one of the most widely known cannabinoids, there are several kinds, and also just just recently have actually significant resources been poured into their research..CBD Massage Oil.MADE IN USA: An all-natural massage oil made from the finest ingredients . To extract out and characterize a simple organic compound (a terpene) from oranges via steam distillation. Limonene a volatile oil was extracted from orange peel using soxhlet e xtractor. This is called food grade d-limonene which is 96% to 97% pure and has a mild orange aroma. ()--Pinene 112089. H2NC6H4CO2C2H5, Drugs, Path Length = 10 cm = 1 dm, [] = / (cl), where c is the concentration in g/mL and l is the path length in dm Experiment II: Steam Distillation: Isolation of Limonene from Orange Peels Purpose. This is most likely due Mass (g) 0. x[dWu4mYs/I8DDZL9L$M>LW D_4i^4a?6>wuWZoxXxEp^}56a3p7m~bBabe|x^oo{<>otgi Limonene is also combustible and hence can be used as a fuel. Heat the flask so that distillation proceeds at a steady rate, approximately one drop per second of distillate. The premise: create a removable filter using copper wire and filter paper to jam into the bottom of a disposable centrifuge tube. Limonene can be extracted by various conventional methods like steam distillation cold press, solvent extraction, novel methods like super critical CO2 extraction, it means varied typical ways like steam distillation cold press, solvent extraction, novel ways like super essential greenhouse emission extraction. isoprene units), diterpenes (four isoprene units), and triterpenes (six isoprene units). Rewrite the STEAM DISTILLATION procedure in your own words! Today you will isolate a natural product, specifically, a terpenoid (or terpene) called limonene from the skin of an orange or grapefruit. Extracting limonene from oranges by steam distillation. 1 The reason that CO 2 is used Characterization. Results turned out quite positive: Amount of orange peels used/g as possible the morning of.! You can download the paper by clicking the button above. -do not Is the category for this document correct. Methods: The essential oil (EO) isolated by hydro-distillation from the peel of fully matured ripen fruits of Citrus limettioides Tanaka and analysed by Gas Chromatography-Mass Spectrometry (GC-MS). of the specific rotation we obtained was 79 degrees. The value, of the specific rotation we obtained was 79.05 degrees. Aim: The present study is aimed to isolate the essential oil of Citrus limettioides and analyze its chemical composition and antimicrobial potential. of the Chemical Society of JapanAnnual Research Report of the Florida Agricultural Experiment Station, Institute of Food and Agricultural Sciences, University of Florida, . filtered again if desired (2). Supercritical carbon dioxide extraction technology facilitates the uniform bed that allows reasonable heat and mass transfer as the surface area of the grounded orange peels either wet and/or dried increase the surface area for better penetration of the fluid under sub/supercritical conditions of set parameters. P. Giampaoli, Martine Decloux, Julien Delarue, Innovative Food Science & Emerging Technologies, Food Science and Technology International, Journal of the Brazilian Chemical Society, Supercritical carbon dioxide extraction of volatile oil from Italian coriander seeds, Handbookoffruitsandfruitprocessing-121109232115-phpapp02, Industrial Use of Medicinal and Aromatic Plants Industrial use of Medicinal and Aromatic Plants (MAPs), Supercritical and subcritical carbon dioxide extraction of Indian orange peel oil, Essential Oil of Grape Fruit (Citrus paradisi) Peels and Its Antimicrobial Activities, Chemical Composition and Antimicrobial Activity of Essential Oil of Citrus limettioides Tanaka, Essential Oil of Grape Fruit (<i>Citrus paradisi</i>) Peels and Its Antimicrobial Activities, Identification of key aroma compounds from bitter orange (Citrus aurantium L.) products: essential oil and macerate-distillate extract, Citrus hydrosols as useful by-products for tyrosinase inhibition, High Solid Loading in Dilute Acid Hydrolysis of Orange Peel Waste Improves Ethanol Production, Analysis of Bioactive Compounds in Seven Citrus Cultivars, Comparative Evaluation of Physiochemical and GC-MS Analysis of Sour Oranges and Sweet Oranges Peels Oil Comparative Evaluation of Physiochemical and GC-MS Analysis of Sour Oranges and Sweet Oranges Peels Oil, Flavouring of Dehydrated Convenience Food and Kitchen Aids, Waste to wealth: Industrial raw materials potential of peels of Nigerian sweet orange (Citrus sinensis), Supercritical Carbon Dioxide Extraction of Indian Orange Peel Oil and Hydro Distillation Comparison on Their Compositions, Supercritical CO2 extraction of essential oil from Kabosu (Citrus sphaerocarpa Tanaka) peel, Ionic liquids and fragrances direct isolation of orange essential oil, Citrus Essential Oils: Extraction and Deterpenation, Nanocellulose and Bioethanol Production from Orange Waste using Isolated Microorganisms, Improvement of biogas production from orange peel waste by leaching of Limonene, Succinic acid production from orange peel and wheat straw by batch fermentations of Fibrobacter succinogenes S85, Dewatering and Extraction of Hydrophilic Solutes and Essential Oils from Cryo- preserved Lemon Peels Using Liquefied Dimethyl Ether, Special Report Enzyme-assisted extraction of bioingredients, ETHANOL PRODUCTION FROM ORANGE WASTE WITH A FOCUS ON ITS CELLULOSIC FRAGMENT, Comparison of heat and mass transfer of different microwave-assisted extraction methods of essential oil from Citrus limon (Lisbon variety) peel, A Review of Genetic Taxonomy, Biomolecules Chemistry and Bioactivities of Citrus hystrix DC, RECOVERY OF OIL AND PECTIN FROM CITRUS LIMETTA, Insecticidal potential of grapefruit and tangerine peel essential oils extracted by steam distillation, Utilization of Essential Oil and Pectin Extracted from Nigerian Orange Peels, Send Orders for Reprints to reprints@benthamscience.net Current and Potential Use of Citrus Essential Oils, Essential oil chemical composition and Antimicrobial Activity of Sour Oranges (Citrus aurantium) Peels, extraction of pectin from orange peel for fresh cut fruits edible coating, Pectinase Production From Aspergillus niger And Activity Assay With Pectin Isolated From Orange Peel, EXTRACTION METHODS OF NATURAL ESSENTIAL OILS, Converting citrus wastes into value added products: Economical and environment-friendly approaches, Citrus essential oils: Extraction, authentication and application in food preservation, Valorization of citrus by-products using Microwave Steam Distillation (MSD), EXTRACTION OF D- LIMONENE FROM ORANGE PE (1).

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